Record the stable zero air response as “Z”. ; Walega, J.G. Verify that the photometer manufacturer has adequately established that the linearity error of the photometer is less than 3%, or test the linearity by dilution as follows: Generate and assay an O3 concentration near the upper range limit of the system or appropriate calibration scale for the instrument, then accurately dilute that concentration with zero air and re-assay it. /Resources 3 0 R WASTE MINIMISATION AND MANAGEMENT PLAN TEMPLATE APPENDIX D - 9 1.5 “INDIATIVE IN SIZES” PROVIDES OUNIL’S STANDARD IN SIZES Construction Design (All Types of Developments) Outline how measures for waste avoidance have been incorporated into the design, material purchasing and construction techniques of the development: The length of the light path through the absorption cell must be known with an accuracy of at least 99.5%. 4.5.2.1 Instruction manual. Air Waste Manage. It is part of an overall Gateway Review Framework and measures progress and recommendations in terms of seven focus areas for ICT projects in NSW. The dynamic calibration system may be modified as shown in Figure 3 to allow for dilution air to be metered in downstream of the O3 generator. /Parent 2 0 R i. (See Reference 13 for guidance.). ... Validation and Reconciliation with DQIs. Laboratory Quality Control Frequency of Analysis Measurement Quality Objective Calibration Standard Per analytical method or manufacturer’s specifications Per analytical method or manufacturer’s specifications Continuing Calibration Verification 4.3.3 Ozone generator. Service or replace filters and zero air scrubbers or other consumable materials, as necessary. ... Validation and Reconciliation with DQIs. Additional quality assurance procedures and guidance are provided in 40 CFR part 58, appendix A, and in Reference 14. %����� Repeat at several different dilution ratios. Appendix D Quality Assurance Project Plan 7 Appendix E Health and Safety Plan 7 NOTES for SSI Workplan (beyond PEA): 1. 4.3.1 UV photometer. A number of advantages are realized by locating the calibration photometer in a clean laboratory where it can be stationary, protected from the physical shock of transportation, operated by a responsible analyst, and used as a common standard for all field calibrations via transfer standards. 8.0 Quality Objectives & Criteria for Measurement Data 6. Version Version issue date Author Approval Pages Filename 11 29-Mar-19 NIST QM WGC 1 of 85 NIST QM-I-V11 controlled revised 3_29_19.docx K. H. Becker, U. Schurath, and H. Seitz, “Ozone Olefin Reactions in the Gas Phase. I: Example of Reports to Management . A manual or automatic two-way valve, or other means is used to switch the photometer flow between zero air and the O3 concentration. >> Transfer Standards for Calibration of Ambient Air Monitoring Analyzers for Ozone, EPA publication number EPA-454/B-13-004, October 2013. Section IV. This is only an example, each organisation will have its own objectives. 4.5.5.1 Allow sufficient time for the O3 analyzer and the photometer or transfer standard to warm-up and stabilize. and measurement efforts mandated or supported by EPA have in place a centrally managed Quality Assurance (QA) Program Plan. 3.1 Except as described in 3.2 below, the chemiluminescence measurement system is inherently free of significant interferences from other pollutant substances that may be present in ambient air. Upon initial operation of the photometer, the following steps must be carried out with all quantitative results or indications recorded in a chronological record, either in tabular form or plotted on a graphical chart. EPA, Office of Air Quality Planning and Standards, Research Triangle Park, NC 27711. >> endobj The applicant is to include expected product field performance based on previous data collection, including but not limited A procedure for generating suitable zero air is given in Reference 13. The system must have a vent designed to insure atmospheric pressure in the manifold and to prevent ambient air from entering the manifold. 1 Goal Statements & Objective Statements 6. APPENDIX D CONTENT OF PROJECT PLAN DOCUMENTS D.1 Introduction ... of a project plan document since it is closely associated with the data quality objective (DQO) ... D Data Validation and Usability ; D1 Verification and Validation Requirements : D5.1: 8 : D2 : 4.5.2 Preparation. A. Clyne and J. If substantial adjustment of the span control is necessary, recheck the zero and span adjustments by repeating steps 4.5.5.2 to 4.5.5.4. A device to indicate barometric pressure must be used that is accurate to ±2 torr. 8.0 Quality Objectives & Criteria for Measurement Data 6. (This can be readily achieved by prudent selection of optical filter and detector response characteristics.) 5.1 The frequency of calibration, as well as the number of points necessary to establish the calibration curve, and the frequency of other performance checking will vary by analyzer; however, the minimum frequency, acceptance criteria, and subsequent actions are specified in Appendix D of Reference 14: Measurement Quality Objectives and Validation Templates. /XIPLAYER_CM3 11 0 R Appendix D - Quality Management Plan assessment checklist. 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